US3560627A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Furnace assembly for thermal analysis use
Assignee: Dow Chemical Co
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Filing: 1969-08-07
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Granted: 1971-02-02
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Expires: 1989-08-07
Abstract
Abstract This invention relates to a heating furnace assembly which is adapted to be coupled to and become a part of a mass spectrometer adjacent to the ion source (usually) within the instrument. The furnace is a radiant heating device utilizing glow bar-type heating rods, with or without an adjacent reflective surface and is adapted to be controlled by means of temperature sensing means disposed within a separate thermal analysis cell which is adapted to be disposed within the furnace.
Inventors
- 👤 Horst G Langer
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-03 09:52
CPC Classifications
H; H01; H01J; H01J49/00; H01J49/02; H01J49/04; H01J49/0468; F; F27; F27D; F27D11/00; F27D11/02
Claims Analysis
Total Claims: 7
Claim 1
Independent Claim
216 words
A furnace and sample insertion assembly for use under high vacuum conditions, comprising first tubular means, a first disc having a central bore which is at least as large as the inner diameter of said first tubular means, said first disc being disposed perpendicularly with respect to said first tubular means and secured thereto an array of rodlike heating elements electrically coupled and disposed perpendicularly with respect to said first disc and secured adjacent to the outer periphery of said first disc, a second disc, said second disc being disposed above said first disc and electrically and mechanically coupled to said heating elements, a second tubular element, said second tubular element being axially aligned with a flanged mounting plate, said flanged plate extending transversely from said tubular element means intermediate the ends thereof, said flanged plate being hermetically sealed to said tubular element means, said tubular means having a valve therein on the side of said flanged plate remote from said rodlike heating elements, said tubular element having an inner diameter which is slightly larger than the diameter of a thermal analysis cell assembly adapted to be inserted therethrough and into the space within said rodlike heating elements, means for sealing the tubing means to said cell assembly, and lead means for energizing said heater winding.
Claim 2
Dependent Claim
216 words
A furnace and sample insertion assembly for use under high vacuum conditions, comprising first tubular means, a first disc having a central bore which is at least as large as the inner diameter of said first tubular means, said first disc being disposed perpendicularly with respect to said first tubular means and secured thereto an array of rodlike heating elements electrically coupled and disposed perpendicularly with respect to said first disc and secured adjacent to the outer periphery of said first disc, a second disc, said second disc being disposed above said first disc and electrically and mechanically coupled to said heating elements, a second tubular element, said second tubular element being axially aligned with a flanged mounting plate, said flanged plate extending transversely from said tubular element means intermediate the ends thereof, said flanged plate being hermetically sealed to said tubular element means, said tubular means having a valve therein on the side of said flanged plate remote from said rodlike heating elements, said tubular element having an inner diameter which is slightly larger than the diameter of a thermal analysis cell assembly adapted to be inserted therethrough and into the space within said rodlike heating elements, means for sealing the tubing means to said cell assembly, and lead means for energizing said heater winding.
Claim 3
Dependent Claim
23 words
An assembly in accordance with claim 1, wherein said means for sealing the tubing means to said cell assembly comprises a compression seal.
Claim 4
Dependent Claim
33 words
An assembly in accordance with claim 1, wherein a heat reflective surface is disposed adjacent to each of said rodlike heating elements and each presents a concave surface to its rodlike heating element.
Claim 5
Dependent Claim
17 words
An assembly in accordance with claim 1, wherein a sleeve extends between said first and second discs.
Claim 6
Dependent Claim
20 words
An assembly in accordance with claim 1, wherein said flanged plate is adapted to be coupled to a mass spectrometer.
Claim 7
Dependent Claim
16 words
An assembly in accordance with claim 4, wherein said sleeve has a heat reflective inner surface.
References Cited (Backward Citations)
US2971039A
Cited
US3257492A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1974-02-01 | 1974-08-03 | 1975-02-02 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1978-02-01 | 1978-08-03 | 1979-02-02 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1982-02-01 | 1982-08-03 | 1983-02-02 | $7700.00 | Window Closed / Lapsed |