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US3559703A Expired / Lapsed US ⏱️ 0.0 years remaining

Fluid sample injector for gas chromatograph

Assignee: Citgo Petroleum Corp
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Filing: 1969-05-29
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Granted: 1971-02-02
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Expires: 1989-05-29
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Abstract

Abstract A fluid sample to be analyzed is delivered to a fluid analyzing instrument, e.g. a gas chromatography column, by delivery through conduit means to a passageway inside a housing removably secured to the fluid analyzing instrument. Interconnecting with this passageway is a second passageway extending from the outer end of the housing to the end thereof secured to the instrument. This second passageway is aligned with the point at which the fluid may be injected into the fluid analyzing instrument. A syringetype device having a needle adapted to fit in this second passageway and having a sufficient length to extend therethrough into the fluid analyzing instrument is provided. In order to prevent the venting of the fluids delivered to the interconnecting passageways, thereby affecting the composition of the fluid to be analyzed, sealing means, such as a rubber pad, is provided and positioned across the second passageway extending to the outermost end thereof. The needle may be inserted into the passageway by penetrating the sealing means, which has a selfsealing character so as to form a tight seal about the needle passing therethrough. In order to prevent the uncontrolled flow of fluids to the gas analyzing instrument, sealing means are also provided between the housing and the instrument and are positioned across the passageway extending therebetween. The needle, containing the desired quantity of the fluid to be analyzed, may be passed through the sealing means into the gas injection point of the instrument. The housing is conveniently formed in three parts, an intermediate cell having the interconnecting passageways extending therethrough, an inner end cap removably secured to this cell and the instrument and having a passageway extending therethrough in alignment with the end to end passageway in the cell, and an outer end cap removably secured to said cell and also having a passageway extending therethrough in alignment with the end-to-end passageway extending through the cell. The sealing means across the passageway extending from end to end of this three-part housing are positioned between the outer end cap and the cell, between the cell and the inner end cap, and between the inner end cap and the fluid analyzing instrument. Thus, a fluid sample delivered to the passageways in this fluid injector device may be passed therefrom into the analyzing instrument by means of the needle portion of the syringe-type device without any change in composition, so that the results of the fluid analyzing operation will accurately reflect the composition of the gas being analyzed.

Inventors

  • 👤 Robert V Maul
  • 👤 Everett L Swalley

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 04:01
CPC Classifications
G; G01; G01N; G01N30/00; G01N30/02; G01N30/04; G01N30/16; G01N30/18

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 362 words
An apparatus for the injection of a fluid sample into a fluid analyzing instrument comprising: a. a housing removably secured to said fluid analyzing instrument, said housing having passageways therein, the first passageway extending from end-to-end and being in alignment with the fluid injection poinT of the instrument at the end of the housing secured to said instrument, the second passageway interconnecting with said first passageway within the housing and being adapted to receive a sample of the fluid to be analyzed; b. first conduit means for delivering a supply of the fluid to be analyzed to the second passageway of said housing; c. a syringe-type device having a needle portion thereof capable of insertion in said first passageway, said needle being of sufficient length to permit insertion therethrough into the gas analyzing instrument at the fluid injection point thereof, said device also having a plunger means capable of movement between a fluid collecting position in which fluid is drawn into said needle and a fluid expelling position in which fluid is forced from said needle; d. first sealing means contacting said housing and positioned across said first passageway so as to prevent the fluid that enters said housing through said second passageway from venting to the atmosphere through said first passageway, said sealing means being penetrable by said needle and of a self-sealing character so as to form a tight seal about the needle inserted therethrough; and e. second sealing means contacting said housing and positioned across said first passageway so as to prevent the uncontrolled movement of fluid therefrom into said fluid analyzing instrument, said second sealing means being penetrable by said needle and of a self-sealing character so as to form a tight seal about the needle inserted therethrough into said instrument whereby, a representative sample of the fluid to be analyzed may be delivered to the interior of said housing and passed, by means of said needle, into the fluid analyzing instrument without change in composition due to a loss of a portion thereof to the atmosphere, thereby assuring that the analysis of the sample in said instrument accurately reflects the composition of the fluid to be analyzed.
Claim 2
Independent Claim 362 words
An apparatus for the injection of a fluid sample into a fluid analyzing instrument comprising: a. a housing removably secured to said fluid analyzing instrument, said housing having passageways therein, the first passageway extending from end-to-end and being in alignment with the fluid injection poinT of the instrument at the end of the housing secured to said instrument, the second passageway interconnecting with said first passageway within the housing and being adapted to receive a sample of the fluid to be analyzed; b. first conduit means for delivering a supply of the fluid to be analyzed to the second passageway of said housing; c. a syringe-type device having a needle portion thereof capable of insertion in said first passageway, said needle being of sufficient length to permit insertion therethrough into the gas analyzing instrument at the fluid injection point thereof, said device also having a plunger means capable of movement between a fluid collecting position in which fluid is drawn into said needle and a fluid expelling position in which fluid is forced from said needle; d. first sealing means contacting said housing and positioned across said first passageway so as to prevent the fluid that enters said housing through said second passageway from venting to the atmosphere through said first passageway, said sealing means being penetrable by said needle and of a self-sealing character so as to form a tight seal about the needle inserted therethrough; and e. second sealing means contacting said housing and positioned across said first passageway so as to prevent the uncontrolled movement of fluid therefrom into said fluid analyzing instrument, said second sealing means being penetrable by said needle and of a self-sealing character so as to form a tight seal about the needle inserted therethrough into said instrument whereby, a representative sample of the fluid to be analyzed may be delivered to the interior of said housing and passed, by means of said needle, into the fluid analyzing instrument without change in composition due to a loss of a portion thereof to the atmosphere, thereby assuring that the analysis of the sample in said instrument accurately reflects the composition of the fluid to be analyzed.
Claim 3
Dependent Claim 178 words
The apparatus of claim 1 in which said housing comprises: a. a cell having said interconnecting passageway therein, the first passageway extending from end to end thereof and the second passageway being adapted to receive a sample of the fluid to be analyzed; b. an inner end cap removably secured to said cell and to said instrument, said inner cap having a passageway therethrough in alignment with said first passageway of the cell and also in with the fluid injection point of said instrument; and c. an outer end cap removably secured to said cell, said outer end cap having a passageway therethrough in alignment with said first passageway through said cell, said first sealing means being placed between said cell and said outer end cap and positioned across the passageway extending therebetween so as to prevent the venting of fluids to the atmosphere, and said second sealing means being placed between said cell and inner end cap and positioned across said passageway extending therebetween so as to prevent the uncontrolled flow of fluid into said analyzing instrument.
Claim 4
Dependent Claim 72 words
The apparatus of claim 2 in which said second passageway in said cell extends from side to side therein and including second conduit means for discharging fluids from said passageway and including valve means for controlling the flow of fluids through said second conduit means, whereby the passageways in said housing may be purged so as to assure that a representative sample of the fluids being analyzed is contained within said housing.
Claim 5
Dependent Claim 53 words
The apparatus of claim 3 and including third sealing means placed between said cell and said inner end cap and positioned across said first passageway extending therebetween, said third sealing means being penetrable by said needle and of a self-sealing character so as to form a tight seal about the needle inserted therethrough.
Claim 6
Dependent Claim 28 words
The apparatus of claim 2 and including valve means positioned in said first conduit means for controlling the delivery of fluids to said second passageway in said cell.
Claim 7
Dependent Claim 17 words
The appaRatus of claim 4 and including mechanical means for securing said syringe-type device to said housing.
Claim 8
Dependent Claim 57 words
The apparatus of claim 1 in which said syringe-type device has a calibration scale associated therewith so that the amount of fluid drawn into said needle by movement of said plunger means into a fluid collecting position may readily be observed, facilitating the injection of a desired volume of the sample to be analyzed into said instrument.
Claim 9
Dependent Claim 72 words
The apparatus of claim 7 and including stop means attached to the mechanical means for securing said syringe-type device to said housing, said stop means being positioned so as to limit the movement of said plunger means to a predetermined point so as to facilitate the collecting of a predetermined quantity of fluid in said needle and subsequently expelling said predetermined quantity of fluid from said needle into said fluid analyzing instrument.
Claim 10
Dependent Claim 26 words
The apparatus of claim 1 in which said first and second sealing means comprise rubber pads capable of maintaining pressure-tight seals around said needle inserted therethrough.
Claim 11
Dependent Claim 28 words
The apparatus of claim 4 in which said first, second and third sealing means comprise rubber pads capable of forming a pressure-tight seal around said needle inserted therethrough.

References Cited (Backward Citations)

No citation records indexed.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1974-02-01 1974-08-03 1975-02-02 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1978-02-01 1978-08-03 1979-02-02 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1982-02-01 1982-08-03 1983-02-02 $7700.00 Window Closed / Lapsed

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