Method for preparing secondary aminothiazoledisulfides

Claim 1

THE METHOD FOR PREPARING SECONDARY AMINOBENZOTHIAZOLEDISULFIDES COMPRISING REACTING SUBSTANTIALLY TWO MOLES OF A 2-MERCAPTOBENZOTHIAZOLE SELECTED FROM THE GROUP CONSISTING OF 2-MERCAPTOBENZOTHIAZOLE, 4-PHENYL2-MERCAPTOBENZOTHIAZOLE, 6-PHENYL-2-MERCAPTOBENZOTHIAZOLE, 4-METHYL-2-MERCAPTOBENZOTHIAZOLE, 6-METHYL-2MERCAPTOBENZOTHIAZOLE AND 2-MERCAPTOTETRAHYDROBENZOTHIAZOLE AND SUBSTANTIALLY SIX MOLES OF A SECONDARY AMINE SELECTED FROM THE GROUP CONSISTING OF MORPHOLINE AND 2,6-DIMETHYL MORPHOLINE WITH SUBSTANTIALLY ONE MOLE OF CHLORINE AT A TEMPERATURE OF FROM ABOUT 0*C. TO ABOUT 30*C. AND THEN REACTING THE PRODUCT WITH SUBSTANTIALLY ONE MOLE OF A SULFUR MONOHALIDE SELECTED FROM THE GROUP CONSISTING OF SULFUR MONOCHLORIDE, SULFUR MONOBROMIDE AND SULFUR MONOIODIDE AT A TEMPERATURE OF FROM ABOUT 40*C. TO ABOUT 100*C. IN AN INERT ORGANIC DILUENT SELECTED FROM THE GROUP CONSISTING OF TOLUENE, BENZENE, CHLOROFORM AND CHLOROBENZENE.

Claim 2

THE METHOD FOR PREPARING SECONDARY AMINOBENZOTHIAZOLEDISULFIDES COMPRISING REACTING SUBSTANTIALLY TWO MOLES OF A 2-MERCAPTOBENZOTHIAZOLE SELECTED FROM THE GROUP CONSISTING OF 2-MERCAPTOBENZOTHIAZOLE, 4-PHENYL2-MERCAPTOBENZOTHIAZOLE, 6-PHENYL-2-MERCAPTOBENZOTHIAZOLE, 4-METHYL-2-MERCAPTOBENZOTHIAZOLE, 6-METHYL-2MERCAPTOBENZOTHIAZOLE AND 2-MERCAPTOTETRAHYDROBENZOTHIAZOLE AND SUBSTANTIALLY SIX MOLES OF A SECONDARY AMINE SELECTED FROM THE GROUP CONSISTING OF MORPHOLINE AND 2,6-DIMETHYL MORPHOLINE WITH SUBSTANTIALLY ONE MOLE OF CHLORINE AT A TEMPERATURE OF FROM ABOUT 0*C. TO ABOUT 30*C. AND THEN REACTING THE PRODUCT WITH SUBSTANTIALLY ONE MOLE OF A SULFUR MONOHALIDE SELECTED FROM THE GROUP CONSISTING OF SULFUR MONOCHLORIDE, SULFUR MONOBROMIDE AND SULFUR MONOIODIDE AT A TEMPERATURE OF FROM ABOUT 40*C. TO ABOUT 100*C. IN AN INERT ORGANIC DILUENT SELECTED FROM THE GROUP CONSISTING OF TOLUENE, BENZENE, CHLOROFORM AND CHLOROBENZENE.