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US2889221A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of producing titanium

Assignee: National Research Corp
•
Filing: 1952-05-03
•
Granted: 1959-06-02
•
Expires: 1972-05-03
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Abstract

No abstract record available.

Inventors

  • 👤 Richard H Singleton

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-26 22:17
CPC Classifications
C; C22; C22B; C22B34/00; C22B34/10; C22B34/12; C22B34/129; C22B5/00; C22B5/02; C22B5/04; C22B5/06

Claims Analysis

Total Claims: 2
Claim 1
Independent Claim 189 words
THE PROCESS OF FORMING TITANIUM WHICH COMPRISES PASSING TITANIUM TRICHLORIDE THROUGH FIRST DISPROPORTIONATION ZONE WHILE HEATING SAID TITANIUM TRICHLORIDE TO A TEMPERATURE SUFFICIENT TO DISPROPORTIONATE A SUBSTANTIAL AMOUNT OF SAID TRICHLORIDE TO THE DICHLORIDE, CONTINUOUSLY REMOVING TITANIUM TETRACHLORIDE FROM THE FIRST DISPROPORTIONATION ZONE SO AS TO MAINTAIN THE PATIAL PRESSURE OF TITANIUM TETRACHLORIDE BELOW THE EQUILBRIUM DISPROPORTIONATION PRESURE OF TITANIUM TRICHLORIDE AT THE TEMPERATURE OF THE TRICHLORIDE IN THE FIRST DISPROPORTIONATION ZONE, PASSING THE NONVOLATILE PRODUCT FROM THE FIRST DISPROPORTIONATION ZONE INTO AND THROUGH A SECOND DISPROPORTIONATION ZONE WHEREIN THE SAID NONVOLATILE PRODUCT IS HEATED TO A TEMPERATURE ON THE ORDER OF 1000*C. TO 1400*C. TO OBTAIN TITANIUM METAL, MAINTAINING THE PARTIAL PRESSURE OF THE GASEOUS TITANIUM CHLORIDES IN THE SECOND DISPROPORTIONATION ZONE BELOW THE EQUILIBRIUM DISPROPORTIONATION PRESSURE OF TITANIUM DICHLORIDE AT THE TEMPERATURE OF TITANIUM DICHLORIDE IN THE SECOND DISPROPORTIONATION ZONE, CONTINUOUSLY WITHDRAWING THE TITANIUM CHLORIDE VAPORS GENERATED IN THE SECOND ZONE, PASSING SAID VAPORS COUNTERCURRENT TO THE FLOW OF, AND IN CONTACT WITH, THE SOLID TITANIUM CHLORIDES ADVANCING THROUGH THE TWO DISPROPORTIONATION ZONES, AND CONDENSING TITANIUM TRICHLORIDE FROM THESE COUNTERFLOWING TITANIUM CHLORIDE VAPORS IN THE FIRST ZONE.
Claim 2
Dependent Claim 189 words
THE PROCESS OF FORMING TITANIUM WHICH COMPRISES PASSING TITANIUM TRICHLORIDE THROUGH FIRST DISPROPORTIONATION ZONE WHILE HEATING SAID TITANIUM TRICHLORIDE TO A TEMPERATURE SUFFICIENT TO DISPROPORTIONATE A SUBSTANTIAL AMOUNT OF SAID TRICHLORIDE TO THE DICHLORIDE, CONTINUOUSLY REMOVING TITANIUM TETRACHLORIDE FROM THE FIRST DISPROPORTIONATION ZONE SO AS TO MAINTAIN THE PATIAL PRESSURE OF TITANIUM TETRACHLORIDE BELOW THE EQUILBRIUM DISPROPORTIONATION PRESURE OF TITANIUM TRICHLORIDE AT THE TEMPERATURE OF THE TRICHLORIDE IN THE FIRST DISPROPORTIONATION ZONE, PASSING THE NONVOLATILE PRODUCT FROM THE FIRST DISPROPORTIONATION ZONE INTO AND THROUGH A SECOND DISPROPORTIONATION ZONE WHEREIN THE SAID NONVOLATILE PRODUCT IS HEATED TO A TEMPERATURE ON THE ORDER OF 1000*C. TO 1400*C. TO OBTAIN TITANIUM METAL, MAINTAINING THE PARTIAL PRESSURE OF THE GASEOUS TITANIUM CHLORIDES IN THE SECOND DISPROPORTIONATION ZONE BELOW THE EQUILIBRIUM DISPROPORTIONATION PRESSURE OF TITANIUM DICHLORIDE AT THE TEMPERATURE OF TITANIUM DICHLORIDE IN THE SECOND DISPROPORTIONATION ZONE, CONTINUOUSLY WITHDRAWING THE TITANIUM CHLORIDE VAPORS GENERATED IN THE SECOND ZONE, PASSING SAID VAPORS COUNTERCURRENT TO THE FLOW OF, AND IN CONTACT WITH, THE SOLID TITANIUM CHLORIDES ADVANCING THROUGH THE TWO DISPROPORTIONATION ZONES, AND CONDENSING TITANIUM TRICHLORIDE FROM THESE COUNTERFLOWING TITANIUM CHLORIDE VAPORS IN THE FIRST ZONE.

References Cited (Backward Citations)

US1306568A Cited
US1310724A Cited
US1173012A Cited
US2362718A Cited
US2402084A Cited
US2543898A Cited
US2564337A Cited
US2618549A Cited
US2706153A Cited
US2618550A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1962-06-01 1962-12-01 1963-06-02 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1966-06-01 1966-12-01 1967-06-02 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1970-06-01 1970-12-01 1971-06-02 $7700.00 Window Closed / Lapsed

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