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EP1160294A2 Expired / Lapsed EP ⏱️ 0.0 years remaining

Method for improving the high and low shear rheology of mineral slurries and the products derived therefrom

Assignee: Imerys Kaolin Inc
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Filing: 2001-05-30
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Granted: —
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Expires: 2021-05-30
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Abstract

Abstract The present invention provides several methods for improving the high and low shear rheology of a substantially grit-free and substantially dispersed particulate slurry using a rotor-stator type mill. The methods are applicable to slurries including a natural mineral, suspensions including a natural mineral, and suspensions including synthetic minerals. The methods of the present invention selectively include performance of one or more of the processes of beneficiation, re-milling, dewatering and re-dispersion, and drying, performed in any one of several sequences as disclosed or suggested herein. The present invention further provides a number slurry products having an improved high and/or low shear rheology that are produced by the performance of different combinations of these methods.

Inventors

  • 👤 Bomi M. Bilimoria

Bibliographic Details

Application Number —
Jurisdiction EP
Data Source google_patents
Last Synchronized 2026-10-24 08:53
CPC Classifications
C; C09; C09C; C09C1/00; C09C1/40; C09C1/42; B; B01; B01F; B01F27/00; B01F27/27; B01F2101/00; B01F2101/30; B01F23/00; B01F23/50; C01; C01P; C01P2004/00; C01P2004/60; C01P2004/61; C01P2006/00; C01P2006/22; C01P2006/60; C01P2006/80

Claims Analysis

Total Claims: 42
Claim 1
Independent Claim 36 words
A method for improving the high and low shear rheology of a substantially grit-free and substantially fluid particulate suspension, the method comprising the step of processing the suspension using a rotor-stator mill to produce a product.
Claim 2
Dependent Claim 16 words
The method of Claim 1 wherein the fluid particulate suspension is a substantially dispersed particulate slurry.
Claim 3
Independent Claim 32 words
The method of Claims 1 or 2 wherein the slurry or suspension is substantially dispersed in a dispersant and water at an alkaline pH before it is milled in the rotor-stator mill.
Claim 4
Dependent Claim 21 words
The method of Claim 3 wherein the dispersant is selected from the group consisting of phosphates, polyacrylates, silicates, sulfonates and ligno-sulfates.
Claim 5
Dependent Claim 25 words
The method of Claim 3 wherein the alkaline substance is selected from the group consisting at least of soda ash, sodium hydroxide and ammonium hydroxide.
Claim 6
Dependent Claim 20 words
The method of Claim 3 wherein the suspension or slurry is substantially dispersed in sodium polyacrylate, soda ash and water.
Claim 7
Dependent Claim 27 words
The method of Claim 3 wherein the suspension or slurry is substantially dispersed at a pH of greater than 6.0, as measured by a in-process pH method.
Claim 8
Dependent Claim 17 words
The method of Claim 3 wherein the suspension or slurry is substantially dispersed at about 10-75% solids.
Claim 9
Dependent Claim 17 words
The method of Claim 3 wherein the suspension or slurry is substantially dispersed at about 55-70% solids.
Claim 10
Independent Claim 21 words
The method of Claims 1 or 2 wherein the suspension or slurry has a maximum particle size of about 325 mesh.
Claim 11
Independent Claim 20 words
The method of Claims 1 or 2 wherein the mill for processing the suspension or slurry is a Kady-type mill.
Claim 12
Independent Claim 27 words
The method of Claims 1 or 2 wherein the mill for processing the suspension or slurry includes a conically shaped stator and a corresponding conically shaped rotor.
Claim 13
Independent Claim 45 words
The method of Claims 1 or 2 wherein the mill for processing the suspension or slurry includes a stator and correspondingly shaped rotor which define a gap that is adjustable to provide optimum efficiency as the suspension or slurry is processed to produce the product.
Claim 14
Independent Claim 18 words
The method of Claims 1 or 2 further comprising the step of beneficiating the suspension or slurry product.
Claim 15
Dependent Claim 17 words
The method of Claim 14 further comprising the step of re-milling the beneficiated suspension or slurry product.
Claim 16
Independent Claim 32 words
The method of Claims 1 or 2 further comprising the step of at least partially beneficiating the suspension or slurry prior to and/or following the step of milling the suspension or slurry.
Claim 17
Independent Claim 30 words
The method of Claims 1 or 2 further comprising the step of at least partially dewatering the suspension or slurry prior to the step of milling the suspension or slurry.
Claim 18
Dependent Claim 25 words
The method of Claim 17 further comprising the step of beneficiating the suspension or slurry prior to the step of dewatering the suspension or slurry.
Claim 19
Independent Claim 39 words
The method of Claims 14, 16 or 18 wherein the step of beneficiating the suspension or slurry product comprises performing at least one process selected from the group consisting of fractionation, flotation, selective flocculation, magnetic separation, grinding and leaching.
Claim 20
Independent Claim 38 words
The method of Claims 14, 16 or 18 further comprising the steps of at least partially dewatering the suspension or slurry product to produce a filter cake and redispersing the filter cake to form a suspension or slurry.
Claim 21
Dependent Claim 15 words
The method of Claim 20 further comprising the step of re-milling the redispersed filter cake.
Claim 22
Dependent Claim 32 words
The method of Claim 20 further comprising the step of removing additional water from the redispersed filter cake by a process selected from the group consisting at least of evaporation and drying.
Claim 23
Dependent Claim 27 words
The method of Claim 20 wherein the step of at least partially dewatering the suspension or slurry yields a dewatered product having up to about 75% solids.
Claim 24
Dependent Claim 21 words
The method of Claim 22 wherein the additional water is removed from the suspension or slurry by the process of evaporation.
Claim 25
Dependent Claim 17 words
The method of Claim 24 further comprising the step of re-milling the evaporated suspension or slurry product.
Claim 26
Dependent Claim 19 words
The method of Claim 24 wherein evaporation yields a suspension or slurry product having at least about 30% solids.
Claim 27
Dependent Claim 19 words
The method of Claim 24 wherein evaporation yields a suspension or slurry product having at least about 60% solids.
Claim 28
Dependent Claim 21 words
The method of Claim 22 wherein the additional water is removed from the suspension or slurry by the process of drying.
Claim 29
Dependent Claim 17 words
The method of Claim 28 wherein drying yields a suspension or slurry product having about 85-100% solids.
Claim 30
Dependent Claim 22 words
The method of Claim 22 wherein the additional water is removed from the suspension or slurry by the process of spray drying.
Claim 31
Dependent Claim 15 words
The method of Claim 30 wherein spray drying yields a product having about 94-100% solids.
Claim 32
Independent Claim 16 words
The method of Claims 14, 16, or 18 wherein the particulate comprises a substantially white pigment.
Claim 33
Independent Claim 15 words
The method of Claims 14, 16 or 18 wherein the particulate comprises a kaolin clay.
Claim 34
Independent Claim 14 words
The method of Claims 14, 16 or 18 wherein the particulate comprises calcium carbonate.
Claim 35
Independent Claim 15 words
The method of Claims 14, 16 or 18 wherein the particulate comprises precipitated calcium carbonate.
Claim 36
Independent Claim 15 words
The method of Claims 14, 16 or 18 wherein the particulate comprises a synthetic silica.
Claim 37
Independent Claim 15 words
The method of Claims 14, 16 or 18 wherein the particulate comprises a synthetic silicate.
Claim 38
Independent Claim 14 words
The method of Claims 14, 16 or 18 wherein the particulate comprises an alumino-silicate.
Claim 39
Dependent Claim 21 words
The method of Claim 2 wherein the substantially grit-free and substantially dispersed particulate slurry is formed by a direct precipitation process.
Claim 40
Dependent Claim 14 words
The method of Claim 14 wherein the suspension or slurry is dewatered and redispersed.
Claim 41
Dependent Claim 15 words
The method of Claim 3 wherein the suspension is substantially dispersed at about 30-75% solids.
Claim 42
Dependent Claim 12 words
A product made by the method of any of the preceding claims.

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