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EP0348690A2 Expired / Lapsed EP ⏱️ 0.0 years remaining

Apparatus and method for plasma treatment of small diameter tubes

Assignee: Becton Dickinson and Co
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Filing: 1989-06-03
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Granted: —
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Expires: 2009-06-03
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Abstract

Abstract An apparatus for generating a plasma in the lumen of a small diameter tube includes a housing (12) having a diaphragm (18) which separates the housing into a first chamber (14) equipped with a gas inbleed (26) assembly and a second chamber (16) connected to a vacuum source. Parallel plate electrodes (58) in the first chamber are encased in a dielectric (42) which prevents substantially all plasma discharge external of a plasma zone between the electrodes. A conduit (64) maintains gas flow between the chambers. A bore (52) through the dielectric includes the plasma zone and receives the tube (54) to be plasma treated. A method for treating the luminal wall of a plastic tube (54) includes positioning a tube in the plasma zone, evacuating the chambers, bleeding a gas into the chambers, and delivering radiofrequency power to the electrodes (58). A long tube may be drawn through the plasma zone, or the dielectric and electrodes may be moved past the tube.

Inventors

  • 👤 David B. Montgomery
  • 👤 Joel L. Williams

Bibliographic Details

Application Number —
Jurisdiction EP
Data Source google_patents
Last Synchronized 2026-10-25 20:59
CPC Classifications
C; C23; C23C; C23C16/00; C23C16/04; C23C16/045; A; A61; A61F; A61F2/00; A61F2/02; A61F2/04; A61F2/06; A61F2/062; C23C16/44; C23C16/50; C23C16/505; C23C16/509

Claims Analysis

Total Claims: 15
Claim 1
Independent Claim 132 words
An apparatus for applying a plasma to an interior wall of a plastic article comprising: a) a housing having first and second chambers separated by a diaphragm defining an aperture for receiving an article to be plasma treated; b) a dielectric within said first chamber having a bore therethrough, said bore including a cavity in the interior of said dielectric and a plasma zone for receiving said article; c) an electrode positioned in said cavity and surrounded by said dielectric in all directions except toward said plasma zone and defining said plasma zone; d) means for opening and sealably closing said housing; e) means for delivering power to said electrode; f) means for conducting a gas to said first chamber; and g) means for connecting said second chamber to a vacuum source.
Claim 2
Independent Claim 132 words
An apparatus for applying a plasma to an interior wall of a plastic article comprising: a) a housing having first and second chambers separated by a diaphragm defining an aperture for receiving an article to be plasma treated; b) a dielectric within said first chamber having a bore therethrough, said bore including a cavity in the interior of said dielectric and a plasma zone for receiving said article; c) an electrode positioned in said cavity and surrounded by said dielectric in all directions except toward said plasma zone and defining said plasma zone; d) means for opening and sealably closing said housing; e) means for delivering power to said electrode; f) means for conducting a gas to said first chamber; and g) means for connecting said second chamber to a vacuum source.
Claim 3
Dependent Claim 19 words
The apparatus of Claim 1 further comprising means for maintaining a pressure differential between said first and second chambers.
Claim 4
Dependent Claim 26 words
The apparatus of Claim 1 further comprising drawing means passing sealably through a top wall of said housing for drawing said article through said plasma zone.
Claim 5
Dependent Claim 27 words
The apparatus in accordance with Claim 1 further comprising a support rail for said article passing through said bore, said dielectric being slidably mounted on said rail.
Claim 6
Independent Claim 110 words
An apparatus for applying a plasma to an interior wall of a non-conductive article comprising: a) a housing enclosing a chamber; b) shielding means within said chamber having a bore therethrough, said bore including a cavity and a plasma zone for receiving an article to be plasma treated; c) generating means for an electromagnetic field in said cavity and surrounded by said shielding means in all directions except toward said plasma zone; d) means for opening and sealably closing said housing; e) means for delivering power to said generating means; f) means for conducting a gas to said chamber; and g) means for connecting said chamber to a vacuum source.
Claim 7
Independent Claim 110 words
An apparatus for applying a plasma to an interior wall of a non-conductive article comprising: a) a housing enclosing a chamber; b) shielding means within said chamber having a bore therethrough, said bore including a cavity and a plasma zone for receiving an article to be plasma treated; c) generating means for an electromagnetic field in said cavity and surrounded by said shielding means in all directions except toward said plasma zone; d) means for opening and sealably closing said housing; e) means for delivering power to said generating means; f) means for conducting a gas to said chamber; and g) means for connecting said chamber to a vacuum source.
Claim 8
Independent Claim 189 words
An apparatus for applying a plasma to the luminal wall of a plastic tube comprising: a) a canister having a side wall, a top wall and a diaphragm, said diaphragm dividing said canister into an upper chamber and a lower chamber and defining an aperture; b) a dielectric within said upper chamber, said dielectric having a bore therethrough, said bore communicating through said aperture with said upper and lower chambers, said bore including a cavity in the interior of said dielectric and a plasma zone for receiving a tube to be plasma treated; c) a plurality of electrodes positioned in said cavity and surrounded by said dielectric in all directions except toward said plasma zone and defining said plasma zone therebetween; d) means for opening and sealably closing said canister; e) a conduit through said diaphragm for maintaining a pressure differential between said upper and lower chambers; f) drawing means passing sealably through said top wall; g) means for delivering electrical power to said electrodes; h) an inbleed assembly for conducting gas into said upper chamber; and i) a nozzle for connecting said lower chamber to a vacuum source.
Claim 9
Independent Claim 189 words
An apparatus for applying a plasma to the luminal wall of a plastic tube comprising: a) a canister having a side wall, a top wall and a diaphragm, said diaphragm dividing said canister into an upper chamber and a lower chamber and defining an aperture; b) a dielectric within said upper chamber, said dielectric having a bore therethrough, said bore communicating through said aperture with said upper and lower chambers, said bore including a cavity in the interior of said dielectric and a plasma zone for receiving a tube to be plasma treated; c) a plurality of electrodes positioned in said cavity and surrounded by said dielectric in all directions except toward said plasma zone and defining said plasma zone therebetween; d) means for opening and sealably closing said canister; e) a conduit through said diaphragm for maintaining a pressure differential between said upper and lower chambers; f) drawing means passing sealably through said top wall; g) means for delivering electrical power to said electrodes; h) an inbleed assembly for conducting gas into said upper chamber; and i) a nozzle for connecting said lower chamber to a vacuum source.
Claim 10
Independent Claim 224 words
An apparatus for applying a plasma to the luminal wall of a plastic tube comprising: a) a housing having a first chamber and a second chamber separated by a diaphragm defining an aperture for receiving a tube to be plasma treated, a first end plate removably affixed to said housing defining said first chamber and a second end plate affixed to said housing and defining said second chamber; b) a dielectric within said first chamber, said dielectric having a bore therethrough, said bore including a cavity in the interior of said dielectric and a plasma zone for receiving said tube; c) a plurality of electrodes positioned in said cavity and surrounded by said dielectric in all directions except toward said plasma zone and defining said plasma zone therebetween; d) mating upper and lower support rails for said tube within said first chamber and passing through said bore, said dielectric being slidably mounted on said rails; e) means for removably mating said upper and lower rails; f) a conduit through said diaphragm for maintaining a pressure differential between said first and second chambers; g) means for moving said dielectric on said rails; h) means for delivering electrical power to said electrodes; i) an inbleed assembly for conducting gas into said first chamber; and j) a nozzle for connecting said second chamber to a vacuum source.
Claim 11
Independent Claim 224 words
An apparatus for applying a plasma to the luminal wall of a plastic tube comprising: a) a housing having a first chamber and a second chamber separated by a diaphragm defining an aperture for receiving a tube to be plasma treated, a first end plate removably affixed to said housing defining said first chamber and a second end plate affixed to said housing and defining said second chamber; b) a dielectric within said first chamber, said dielectric having a bore therethrough, said bore including a cavity in the interior of said dielectric and a plasma zone for receiving said tube; c) a plurality of electrodes positioned in said cavity and surrounded by said dielectric in all directions except toward said plasma zone and defining said plasma zone therebetween; d) mating upper and lower support rails for said tube within said first chamber and passing through said bore, said dielectric being slidably mounted on said rails; e) means for removably mating said upper and lower rails; f) a conduit through said diaphragm for maintaining a pressure differential between said first and second chambers; g) means for moving said dielectric on said rails; h) means for delivering electrical power to said electrodes; i) an inbleed assembly for conducting gas into said first chamber; and j) a nozzle for connecting said second chamber to a vacuum source.
Claim 12
Independent Claim 96 words
A method for treating a luminal wall of a tube with a plasma comprising: a) positioning a tube in a plasma zone adjacent a plurality of electrodes, said electrodes being encased in a dielectric in a housing enclosing a chamber; b) evacuating said chamber; c) bleeding a gas into said chamber, said gas contacting a luminal wall of said tube; and d) delivering radiofrequency power to said electrodes, said power developing an electromagnetic field, said field ionizing said gas in contact with said luminal wall, said ionizing causing a plasma, said plasma treating said luminal wall.
Claim 13
Independent Claim 96 words
A method for treating a luminal wall of a tube with a plasma comprising: a) positioning a tube in a plasma zone adjacent a plurality of electrodes, said electrodes being encased in a dielectric in a housing enclosing a chamber; b) evacuating said chamber; c) bleeding a gas into said chamber, said gas contacting a luminal wall of said tube; and d) delivering radiofrequency power to said electrodes, said power developing an electromagnetic field, said field ionizing said gas in contact with said luminal wall, said ionizing causing a plasma, said plasma treating said luminal wall.
Claim 14
Dependent Claim 16 words
The method in accordance with Claim 29 further comprising drawing said tube through said plasma zone.
Claim 15
Dependent Claim 24 words
The method in accordance with Claim 29 further comprising moving said dielectric having said electrodes encased therein past said tube in said plasma zone.

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