EP0301579A2
Expired / Lapsed
EP
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Photographic photosensitive solution manufacturing method and apparatus
Assignee: Fujifilm Holdings Corp
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Filing: 1988-07-29
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Granted: —
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Expires: 2008-07-29
Abstract
Abstract A method and apparatus for manufacturing photographic photosensitive solution to produce crystals of silver halide emulsion having a uniform size and shape and without substantial waste of expensive Ag<+> solution. Flow control valves for controlling the flow rates of Ag<+> and X<-> solutions are controlled according to a predetermined flow rate or pAg potential program and using output signals of respective flow meters or a pAg potentiometer. The flow control valves are motor-controlled flow control valves for which the rate of change of flow rate with valve stroke is small and linear.
Inventors
- 👤 Yasunori Fuji Photo Film Co. Ltd. Ichikawa
- 👤 Hiroshi Fuji Photo Film Co. Ltd. Ohnishi
- 👤 Akira Fuji Photo Film Co. Ltd. Kojima
- 👤 Akira Fuji Photo Film Co. Ltd. Kato
Bibliographic Details
Application Number
—
Jurisdiction
EP
Data Source
google_patents
Last Synchronized
2026-11-09 10:40
CPC Classifications
G; G03; G03C; G03C1/00; G03C1/005; G03C1/015; B; B01; B01F; B01F35/00; B01F35/20; B01F35/21; B01F35/211; B01F35/2111; B01F35/2132; B01F35/80; B01F35/82; B01F23/00; B01F23/40
Claims Analysis
Total Claims: 12
Claim 1
Independent Claim
84 words
A method for manufacturing photographic photosensitive solution, comprising the steps of: preparing in advance Ag⁺ and X⁻ solutions and supplying said Ag⁺ and X⁻ solutions to respective storage tanks; providing for said storage tanks respective motor-controlled flow control valves having a rate of change of flow rate with valve stroke which is small and linear; and controlling said flow control valves to supply Ag⁺ and X⁻ solution from said storage tanks to a precipitation vessel at rates determined in accordance with a predetermined program.
Claim 2
Independent Claim
84 words
A method for manufacturing photographic photosensitive solution, comprising the steps of: preparing in advance Ag⁺ and X⁻ solutions and supplying said Ag⁺ and X⁻ solutions to respective storage tanks; providing for said storage tanks respective motor-controlled flow control valves having a rate of change of flow rate with valve stroke which is small and linear; and controlling said flow control valves to supply Ag⁺ and X⁻ solution from said storage tanks to a precipitation vessel at rates determined in accordance with a predetermined program.
Claim 3
Dependent Claim
43 words
The method for manufacturing photographic photosensitive solution of claim 1, wherein said program is a flow rate program of the form Q = at² + bt + c, where Q is flow rate, t is time, and a, b and c are constants.
Claim 4
Dependent Claim
66 words
The method for manufacturing photographic photosensitive solution of claim 2, further comprising the step of providing flow meters for measuring flow rates of said Ag⁺ and X⁻ solutions from said storage tanks into said precipitation vessel, and wherein said step of controlling said flow control valves comprises feedback controlling said flow control valves in accordance with output signals from said flow meters and said predetermined program.
Claim 5
Dependent Claim
47 words
The method for manufacturing photographic photosensitive solution of claim 1, wherein said program is a pAg potential program of the form E = ℓt² + mt + n, where E is pAg potential in said precipitation vessel, t is time, and ℓ, m and n are constants.
Claim 6
Dependent Claim
58 words
The method for manufacturing photographic photosensitive solution of claim 4, further comprising the step of providing a pAg potentiometer for measuring a pAg potential in said precipitation vessel, and wherein said step of controlling said flow control valves comprises feedback controlling said flow control valves in accordance with output signals from said pAg potentiometer and said predetermined program.
Claim 7
Independent Claim
264 words
An apparatus for manufacturing a photographic photosensitive solution, comprising: respective raw material storage tanks for storing previously prepared Ag⁺ and X⁻ solutions; a flow control valve connected to an outlet of each of said tanks for controlling an outlet flow rate of each of said Ag⁺ and X⁻ solutions from the respective tanks; a precipitation vessel for adding Ag⁺ and X⁻ solutions received through said flow control valves; means for agitating the added Ag⁺ and X⁻ solutions in said precipitation vessel; and a controller for controlling said flow control valves in accordance with a predetermined program, each of said flow control valves comprising: an electric motor; a feed screw mechanism and coupling plate for converting rotation of said motor into linear motion; a valve shaft connected to said coupling plate for moving said valve shaft vertically; a valve casing having a valve seat formed therein and comprising an inlet-side casing, said valve shaft extending along a central axis of said inlet-side casing, and an outlet side casing merging with said inlet-side casing; a valve body connected to said valve shaft, said valve body comprising a working face in the form of a circular truncated cone tapered towards an outlet of said valve, and a valve head disposed in said outlet-side casing, said valve head being shaped with respect to a valve opening area between a surface of said valve head and said valve seat so that a rate of change of flow rate with valve stroke is small and linear, a valve stroke to fully open said valve seat occurring in said inlet-side opening.
Claim 8
Independent Claim
264 words
An apparatus for manufacturing a photographic photosensitive solution, comprising: respective raw material storage tanks for storing previously prepared Ag⁺ and X⁻ solutions; a flow control valve connected to an outlet of each of said tanks for controlling an outlet flow rate of each of said Ag⁺ and X⁻ solutions from the respective tanks; a precipitation vessel for adding Ag⁺ and X⁻ solutions received through said flow control valves; means for agitating the added Ag⁺ and X⁻ solutions in said precipitation vessel; and a controller for controlling said flow control valves in accordance with a predetermined program, each of said flow control valves comprising: an electric motor; a feed screw mechanism and coupling plate for converting rotation of said motor into linear motion; a valve shaft connected to said coupling plate for moving said valve shaft vertically; a valve casing having a valve seat formed therein and comprising an inlet-side casing, said valve shaft extending along a central axis of said inlet-side casing, and an outlet side casing merging with said inlet-side casing; a valve body connected to said valve shaft, said valve body comprising a working face in the form of a circular truncated cone tapered towards an outlet of said valve, and a valve head disposed in said outlet-side casing, said valve head being shaped with respect to a valve opening area between a surface of said valve head and said valve seat so that a rate of change of flow rate with valve stroke is small and linear, a valve stroke to fully open said valve seat occurring in said inlet-side opening.
Claim 9
Dependent Claim
47 words
The apparatus for manufacturing a photographic photosensitive solution of claim 6, further comprising flow meters for measuring the flow rates through each of said flow control valves, said controller controlling said flow control valves in accordance with output signals from said flow meters and said predetermined program.
Claim 10
Dependent Claim
53 words
The apparatus for manufacturing a photographic photosensitive solution of claim 6, further comprising a pAg potentiometer disposed in said precipitation vessel for measuring a pAg potential in said precipitation vessel, said controller controlling each of said flow control valves in accordance with an output signal from said pAg potentiometer and said predetermined program.
Claim 11
Dependent Claim
18 words
The apparatus for manufacturing a photographic photosensitive solution of claim 6, wherein said valve head is cylindrically shaped.
Claim 12
Dependent Claim
18 words
The apparatus for manufacturing a photographic photosensitive solution of claim 6, wherein said valve head is conically shaped.
References Cited (Backward Citations)
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