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EP0267042A2 Expired / Lapsed EP ⏱️ 0.0 years remaining

Detergent granules and a process for their preparation

Assignee: Unilever PLC
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Filing: 1987-11-06
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Granted: —
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Expires: 2007-11-06
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Abstract

Abstract Detergent powders built with alkali metal carbonate and containing both sodium silicate and a calcium carbonate seed crystal material such as calcite are prepared by granulating a carbonate/silicate base powder with the seed crystal material, ideally in the presence of a liquid binder such as sucrose solution.

Inventors

  • 👤 Robert William Anderson
  • 👤 Peter Mccowan Duggleby
  • 👤 Peter Frederick Garner-Gray
  • 👤 Ian Eric Niven
  • 👤 Timothy John Price
  • 👤 Chandulal Kantilal Ranpuria
  • 👤 Thomas Taylor
  • 👤 Raymond John Wilde

Bibliographic Details

Application Number —
Jurisdiction EP
Data Source google_patents
Last Synchronized 2026-11-05 12:43
CPC Classifications
C; C11; C11D; C11D3/00; C11D3/02; C11D3/04; C11D3/10; C11D3/08; C11D3/12; C11D3/1233; C11D3/16; C11D3/20; C11D3/22; C11D3/221; C11D3/222; C11D3/225

Claims Analysis

Total Claims: 12
Claim 1
Independent Claim 64 words
A granular detergent product comprising: (i) from 3% to 42% of a detergent active material selected from anionic detergent active materials, nonionic detergent active materials, nonionic detergent active materials and mixtures thereof; (ii) from 5% to 56% of sodium carbonate: (iii)from 5% to 30% of sodium silicate; and (iv) from 5% to 40% particulate calcite having a surface area of at least 10 m²/g;
Claim 2
Dependent Claim 64 words
A granular detergent product comprising: (i) from 3% to 42% of a detergent active material selected from anionic detergent active materials, nonionic detergent active materials, nonionic detergent active materials and mixtures thereof; (ii) from 5% to 56% of sodium carbonate: (iii)from 5% to 30% of sodium silicate; and (iv) from 5% to 40% particulate calcite having a surface area of at least 10 m²/g;
Claim 3
Dependent Claim 29 words
wherein said detergent active material, sodium carbonate and sodium silicate are in the form of granulated base powder, said calcite being adhered to the surface of said base powder.
Claim 4
Dependent Claim 29 words
wherein said detergent active material, sodium carbonate and sodium silicate are in the form of granulated base powder, said calcite being adhered to the surface of said base powder.
Claim 5
Dependent Claim 36 words
A granular detergent product according to claim 1 further comprising a binder material which serves to adhere said calcite to said base powder, said binder material being selected from sucrose, sodium carboxymethyl cellulose and nonionic surfactants.
Claim 6
Dependent Claim 35 words
A granular detergent product according to claim 1 further comprising a peracid generating bleach system selected from peracids and mixtures of a peroxybleach with a peracid bleach activator, the product being essentially free of phosphorus.
Claim 7
Dependent Claim 66 words
A process for the preparation of a granular detergent product comprising (i) from 3% to 42% of a detergent active material selected from anionic detergent active materials, nonionic detergent active materials and mixtures thereof; (ii) from 5% to 56% of sodium carbonate; (iii)from 5% to 30% of sodium silicate; and (iv) from 5% to 40% particulate calcite having a surface area of at least 10 m²/g;
Claim 8
Dependent Claim 66 words
A process for the preparation of a granular detergent product comprising (i) from 3% to 42% of a detergent active material selected from anionic detergent active materials, nonionic detergent active materials and mixtures thereof; (ii) from 5% to 56% of sodium carbonate; (iii)from 5% to 30% of sodium silicate; and (iv) from 5% to 40% particulate calcite having a surface area of at least 10 m²/g;
Claim 9
Dependent Claim 44 words
comprising the steps of a) granulating said detergent active material, sodium carbonate and sodium silicate to form a granulated base powder; and b) granulating said granulated base powder with said calcite, to cause said calcite to adhere to the surface of said base powder.
Claim 10
Dependent Claim 44 words
comprising the steps of a) granulating said detergent active material, sodium carbonate and sodium silicate to form a granulated base powder; and b) granulating said granulated base powder with said calcite, to cause said calcite to adhere to the surface of said base powder.
Claim 11
Dependent Claim 32 words
A process according to Claim 4, wherein said granulated base powder is formed by spray-drying an aqueous slurry comprising said detergent active material, sodium carbonate and sodium silicate in a spray-drying tower.
Claim 12
Dependent Claim 27 words
A process according to claim 5, wherein said calcite is simultaneously injected into said spray-drying tower, whereby calcite particules encounter said granulated base powder within said tower.

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