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EP0179670A2 Expired / Lapsed EP ⏱️ 0.0 years remaining

Production of silicon carbide cobweb whiskers

Assignee: Sumitomo Chemical Co Ltd
•
Filing: 1985-10-25
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Granted: —
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Expires: 2005-10-25
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Abstract

Abstract Silicon carbide cobweb whiskers are produced by heating a mixture of silicon dioxide powder, carbon powder and a catalyst composed of at least one of niobium, tantalum and compounds thereof in a non-oxidative gas at a temperature of from 1,400 to 1,900°C.

Inventors

  • 👤 Tadanori Hashimoto
  • 👤 Kazuhiko Nakano
  • 👤 Norio Matsuda

Bibliographic Details

Application Number —
Jurisdiction EP
Data Source google_patents
Last Synchronized 2026-11-04 07:16
CPC Classifications
C; C30; C30B; C30B25/00; C30B25/005; C30B29/00; C30B29/10; C30B29/36

Claims Analysis

Total Claims: 12
Claim 1
Independent Claim 66 words
A method of producing silicon carbide cobweb whiskers by reductive carbonisation of silicon dioxide characterised in that a mixture of a silicon dioxide powder, a carbon powder, and a catalyst composed of at least one of niobium, tantalum and compounds thereof is heated in a non-oxidative gas at a temperature of from 1,400 to 1,900°C, to produce silicon carbide cobweb whiskers among particles of unreacted carbon.
Claim 2
Independent Claim 66 words
A method of producing silicon carbide cobweb whiskers by reductive carbonisation of silicon dioxide characterised in that a mixture of a silicon dioxide powder, a carbon powder, and a catalyst composed of at least one of niobium, tantalum and compounds thereof is heated in a non-oxidative gas at a temperature of from 1,400 to 1,900°C, to produce silicon carbide cobweb whiskers among particles of unreacted carbon.
Claim 3
Dependent Claim 27 words
A method according to claim 1, wherein the amount of carbon powder is from 0.6 to 3 parts per part of said silicon dioxide powder by weight.
Claim 4
Dependent Claim 39 words
A method according to claim 1 or 2, wherein the amount of catalyst is from 0.0001 to 0.1 part, based on the total weight of niobium and tantalum as elements, per part by weight of said silicon dioxide powder.
Claim 5
Dependent Claim 29 words
A method according to claim 1, 2 or 3, wherein the mixture is heated at a temperature of from 1,450 to 1,800°C in an atmosphere of argon and/or hydrogen.
Claim 6
Dependent Claim 29 words
A method according to claim 1, 2 or 3, wherein the mixture is heated at a temperature of from 1,600 to 1,800°C in an atmosphere of a nitrogen-containing gas.
Claim 7
Dependent Claim 14 words
A method according to claim 5, wherein the nitrogen-containing gas is nitrogen and/or ammonia.
Claim 8
Independent Claim 40 words
A method according to any preceding claim, wherein the unreacted carbon is removed by subsequently heating the mixture of silicon carbide cobweb whiskers and unreacted carbon at a temperature of from 600 to 800°C in an atmosphere of oxidative gas.
Claim 9
Dependent Claim 14 words
A method according to claim 7, wherein the oxidative gas is oxygen or air.
Claim 10
Independent Claim 22 words
A method according to any preceding claim, wherein the catalyst is composed of at least one of niobium pentoxide and tantalum pentoxide.
Claim 11
Dependent Claim 14 words
Silicon carbide cobweb whiskers having a mean diameter of from 0.1 to 1.0 µm.
Claim 12
Dependent Claim 14 words
Silicon carbide cobweb whiskers having a mean diameter of from 0.1 to 1.0 µm.

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