EP0080665B1
Expired / Lapsed
EP
⏱️ 0.0 years remaining
Method of producing a flat body from a reactive polymer with high thickness accuracy and consistency
Assignee: BASF SE
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Filing: 1982-11-19
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Granted: 1986-10-22
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Expires: 2002-11-19
Abstract
No abstract record available.
Inventors
- 👤 Albrecht Dr. Eckell
- 👤 Heinz Dr. Pohlemann
- 👤 Christof Dr. Taubitz
- 👤 Lothar Schlemmer
- 👤 Gerhard Bleckmann
Bibliographic Details
Application Number
—
Jurisdiction
EP
Data Source
google_patents
Last Synchronized
2026-10-27 20:20
CPC Classifications
B; B29; B29C; B29C48/00; B29C48/25; B29C48/285; B29C48/29; B29C48/001; B29C48/022; B29C48/36; B29C48/395; B29C48/40; B29C48/405; B29C48/03; B29C48/07; B29C48/08; B29K; B29K2101/00; B29K2101/10; B29K2105/00; B29K2105/0005; B29K2301/00; B29K2301/10
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
282 words
A process for the production of a reactive sheet-like structure which is solid at room temperature and of highly uniform thickness, from a mixture of a thermoplastically processable polymer. a low-viscosity ethylenically unsaturated compound as the crosslinking promoter and a crosslinking assistant. with or withtout further solid and/or liquid additives, by homogeneously mixing the components forming the reactive sheet-like structure, extruding the mixture and shaping the sheet-like structure of the desired thickness by calendering, wherein first of all the thermoplastically processable polymer, with or without additional, in particular solid, constituents of the mixture, is fed into a first zone - viewed in the direction of product flow - of a self-cleaning multi-screw extruder at a temperature below the melting point of the thermoplastically processable polymer, and conveyed into a second zone in which the thermoplastically processable polymer is melted and into which all, or the greater part, of the liquid, low-viscosity constituents of the mixture, and any other constituents which may be used, are then fed. all constituents of the mixture being homogeneously mixed in said zone ; the homogeneous melt is freed from undesirable volatile constituents in a downstream devolatilizing zone, after which the devolatilized melt is discharged from the extruder through a slot die ; and then, in order to obtain the desired thickness, the extruded sheet-like structure is passed directly through the nip of a pair of rolls at a temperature at which the sheet-like structure is at least partially irreversibly deformable under the processing conditions ; and wherein the sheet-like structure extruded through the slot die is fed to the pair of rolls at such a speed that a bank of material forms in front of the nip.
Claim 2
Dependent Claim
282 words
A process for the production of a reactive sheet-like structure which is solid at room temperature and of highly uniform thickness, from a mixture of a thermoplastically processable polymer. a low-viscosity ethylenically unsaturated compound as the crosslinking promoter and a crosslinking assistant. with or withtout further solid and/or liquid additives, by homogeneously mixing the components forming the reactive sheet-like structure, extruding the mixture and shaping the sheet-like structure of the desired thickness by calendering, wherein first of all the thermoplastically processable polymer, with or without additional, in particular solid, constituents of the mixture, is fed into a first zone - viewed in the direction of product flow - of a self-cleaning multi-screw extruder at a temperature below the melting point of the thermoplastically processable polymer, and conveyed into a second zone in which the thermoplastically processable polymer is melted and into which all, or the greater part, of the liquid, low-viscosity constituents of the mixture, and any other constituents which may be used, are then fed. all constituents of the mixture being homogeneously mixed in said zone ; the homogeneous melt is freed from undesirable volatile constituents in a downstream devolatilizing zone, after which the devolatilized melt is discharged from the extruder through a slot die ; and then, in order to obtain the desired thickness, the extruded sheet-like structure is passed directly through the nip of a pair of rolls at a temperature at which the sheet-like structure is at least partially irreversibly deformable under the processing conditions ; and wherein the sheet-like structure extruded through the slot die is fed to the pair of rolls at such a speed that a bank of material forms in front of the nip.
Claim 3
Dependent Claim
25 words
A process as claimed in claim 1, wherein atwin-screw extruder provided with kneading discs and having self-cleaning screws rotating in the same direction is employed.
Claim 4
Dependent Claim
30 words
A process as claimed in claims 1 and 2, wherein the liquid low-viscosity constituents of the mixture are fed into the first two-thirds of the 2nd zone of the extruder.
Claim 5
Dependent Claim
24 words
A process as claimed in claims 1 to 3, wherein the temperature of the devolatilizing zone of the extruder is from 60 to 140°C.
Claim 6
Dependent Claim
62 words
A process as claimed in claims 1 to 4, wherein the first zone of the extruder has a length which is from 2 to 10 times the screw diameter, the second zone has a length which is from 10 to 50 times the screw diameter, and the devolatilizing zone has a length which is from 2 to 20 times the screw diameter.
Claim 7
Dependent Claim
33 words
A process as claimed in claims 1 to 5, wherein the mean residence time of the thermoplastically processable polymer in the extruder is from 1 to 6, preferably from 1.2 to 2.5 minutes.
Claim 8
Dependent Claim
33 words
A process as claimed in claims 1 to 6, wherein a film or foil, on one or both sides of the extruded sheet-like structure, is fed together with the latter through the nip.
Claim 9
Dependent Claim
38 words
A process as claimed 1 to 6, wherein a support which may or may not have been coated with an adhesive is fed together with the extruded sheet-like structure, on one or both sides thereof, through the nip.
Claim 10
Dependent Claim
29 words
A process as claimed in claims 1 to 8, wherein the reactive sheet-like structure, after leaving the nip, has a thickness of from about 10 f.Lm to 6 mm.
References Cited (Backward Citations)
No citation records indexed.
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