CA1100745A
Expired / Lapsed
CA
⏱️ 0.0 years remaining
Smoking materials
Assignee: Gallaher Ltd
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Filing: 1977-10-04
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Granted: 1981-05-12
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Expires: 1997-10-04
Abstract
Abstract "IMPROVEMENTS RELATING TO SMOKING MATERIALS". ABSTRACT OF THE DISCLOSURE The invention is concerned with a tobacco substitute which is made by subjecting a strand of viscose fibres to a controlled pyrolysis until the organic residue contains at least 90% carbon by weight, and loading the carbon strand with ingredients for smoking.
Inventors
- 👤 Jacques Ehretsmann
- 👤 Robert D. Cowling
- 👤 Dennis F. Boyd
- 👤 Alfred D. Schweizer
- 👤 William M. Caldwell
- 👤 Robert J. Boyd
Bibliographic Details
Application Number
—
Jurisdiction
CA
Data Source
google_patents
Last Synchronized
2026-11-02 10:53
CPC Classifications
A; A24; A24B; A24B15/00; A24B15/10; A24B15/16; A24B15/165
Claims Analysis
Total Claims: 21
Claim 1
Independent Claim
87 words
A method of making tobacco substitute smoking product fuel, said method comprising providing a mass of substantially round cross-section, crimped viscose fibres having between 6 and 8 crimps per cm, a denier of between 5 and 20, and a length of between 20 and 100 mm, and subjecting the mass of viscose fibres to controlled pyrolysis until the organic residue contains at least 95% carbon by weight, an oxygen content of between 1 and 4% by weight, and a hydrogen content of less than 1% by weight.
Claim 2
Independent Claim
87 words
A method of making tobacco substitute smoking product fuel, said method comprising providing a mass of substantially round cross-section, crimped viscose fibres having between 6 and 8 crimps per cm, a denier of between 5 and 20, and a length of between 20 and 100 mm, and subjecting the mass of viscose fibres to controlled pyrolysis until the organic residue contains at least 95% carbon by weight, an oxygen content of between 1 and 4% by weight, and a hydrogen content of less than 1% by weight.
Claim 3
Dependent Claim
19 words
Method according to claim 1, wherein the viscose fibres are in the form of a sliver of staple fibres.
Claim 4
Dependent Claim
24 words
Method according to claim 2, wherein the sliver has, after the pyrolysis, a linear density of organic residue of between 1.5 and 7 g/m.
Claim 5
Dependent Claim
91 words
A tobacco substitute smoking product fuel comprising a strand of substantially round cross-section, crimped pyrolysed fibres, the organic residue of which has a linear density of between 1.5 and 7 g/m and which contains at least 95% carbon by weight, an oxygen content of between 1 and 4% by weight, and a hydrogen content of less than 1% by weight, said fibres being the product of controlled pyrolysis of a sliver of staple viscose fibres having a denier between 5 and 20, and a length of between 20 and 100 mm.
Claim 6
Dependent Claim
91 words
A tobacco substitute smoking product fuel comprising a strand of substantially round cross-section, crimped pyrolysed fibres, the organic residue of which has a linear density of between 1.5 and 7 g/m and which contains at least 95% carbon by weight, an oxygen content of between 1 and 4% by weight, and a hydrogen content of less than 1% by weight, said fibres being the product of controlled pyrolysis of a sliver of staple viscose fibres having a denier between 5 and 20, and a length of between 20 and 100 mm.
Claim 7
Independent Claim
120 words
A method of making a tobacco substitute smoking product fuel, said method comprising providing a strand of viscose fibres and subjecting said viscose fibres to controlled pyrolysis until the organic residue contains at least 90% carbon by weight by the stepwise heating of said the strand by passing the strand ?ongitudinally, either continuously or in stepwise manner, through a pyrolysing oven, and therein first raising the temperature of the strand gradually from between 200°C and 300°C to between 400°C and 550°C to dry the strand and provide the majorchemical transformation reactions of the viscose, and thereafter quickly raising the temperature of the strand to between 700°C and 1200°C for long enough to complete the transformation of the viscose to carbon.
Claim 8
Independent Claim
120 words
A method of making a tobacco substitute smoking product fuel, said method comprising providing a strand of viscose fibres and subjecting said viscose fibres to controlled pyrolysis until the organic residue contains at least 90% carbon by weight by the stepwise heating of said the strand by passing the strand ?ongitudinally, either continuously or in stepwise manner, through a pyrolysing oven, and therein first raising the temperature of the strand gradually from between 200°C and 300°C to between 400°C and 550°C to dry the strand and provide the majorchemical transformation reactions of the viscose, and thereafter quickly raising the temperature of the strand to between 700°C and 1200°C for long enough to complete the transformation of the viscose to carbon.
Claim 9
Dependent Claim
29 words
Method according to claim 5, wherein the pyrolysis step is carried out in the oven in the presence of a non-reactive atmosphere which comprises nitrogen, steam, or mixture thereof.
Claim 10
Independent Claim
75 words
A method of making a smoking product for use as a tobacco substitute, said method comprising providing a mass of viscose fibres having a nicotine component carrier, which comprises an alumino silicate, aluminum oxide or silica, homogeneously dispersed therein, thereafter subjecting the mass of viscose fibres to controlled pyrolysis until the organic residue contains at least 90% carbon by weight, and thereafter loading the pyrolysed product with the ingredients for smoking including a nicotine component.
Claim 11
Independent Claim
75 words
A method of making a smoking product for use as a tobacco substitute, said method comprising providing a mass of viscose fibres having a nicotine component carrier, which comprises an alumino silicate, aluminum oxide or silica, homogeneously dispersed therein, thereafter subjecting the mass of viscose fibres to controlled pyrolysis until the organic residue contains at least 90% carbon by weight, and thereafter loading the pyrolysed product with the ingredients for smoking including a nicotine component.
Claim 12
Independent Claim
83 words
A method for making a smoking tobacco substitute product fuel, said method comprising providing a mass of viscose fibres having homogeneously dispersed therein at least one inorganic combustion modifying agent precursor, and subjecting the viscose fibres to controlled pyrolysis until the organic residue contains at least 90% carbon by weight and said inorganic combustion modifying agent precursor is converted into an inorganic combustion modifying agent consisting of calcium carbonate, to produce a pyrolysed product with said inorganic combustion modifying agent homogeneously dispersed therein.
Claim 13
Independent Claim
83 words
A method for making a smoking tobacco substitute product fuel, said method comprising providing a mass of viscose fibres having homogeneously dispersed therein at least one inorganic combustion modifying agent precursor, and subjecting the viscose fibres to controlled pyrolysis until the organic residue contains at least 90% carbon by weight and said inorganic combustion modifying agent precursor is converted into an inorganic combustion modifying agent consisting of calcium carbonate, to produce a pyrolysed product with said inorganic combustion modifying agent homogeneously dispersed therein.
Claim 14
Dependent Claim
10 words
Method of claim 8, wherein said precursor is calcium formate.
Claim 15
Dependent Claim
10 words
Method of claim 8, wherein said precursor is calcium nitrate.
Claim 16
Dependent Claim
22 words
Method of claim 8, wherein said precursor is applied to said viscose fibres in the form of a solution of said precursor.
Claim 17
Dependent Claim
63 words
Method of claim 8, including the additional step of dispersing in said pyrolysed mass, a further combustion modifying agent which is at least one of ammonium dihydrogen phosphate; diammonium hydrogen phosphate; the mono-, di- and tri-phosphate of sodium and potassium; and the meta- and tetra-borates of sodium and potassium, by contacting said pyrolysed product with a solution of said further combustion modifying agent.
Claim 18
Independent Claim
201 words
A method for making a smoking tobacco substitute product fuel, said method comprising providing a mass of viscose fibres, applying calcium formate to said viscose fibres in the form of a calcium formate solution, to homogeneously disperse said calcium formate into said mass, thereafter subjecting said mass to controlled pyrolysis until the organic residue contains at least 90% carbon by weight, and said calcium formate is converted to calcium carbonate, to produce a pyrolysed product with said calcium carbonate homogeneously dispersed therein, and thereafter dispersing in the pyrolysed product a further combustion modifying agent which is at least one of ammonium di- hydrogen phosphate, diammonium hydrogen phosphate, the mono- , di- and tri- phosphates of sodium and potassium, and the meta- and tetra-borates of sodium and potassium, by contacting said pyrolysed product with a solution of said further combustion modifying agent, wherein said calcium formate and said further combustion modifying agent are dispersed on said fibres in said mass by dipping said mass in . a solution of said calcium formate, and subsequently deliquoring and drying said fibres, and by dipping said pyrolysed mass in a solution of said further combustion modifying agent, and subsequently deliquoring and drying said pyrolysed mass.
Claim 19
Independent Claim
201 words
A method for making a smoking tobacco substitute product fuel, said method comprising providing a mass of viscose fibres, applying calcium formate to said viscose fibres in the form of a calcium formate solution, to homogeneously disperse said calcium formate into said mass, thereafter subjecting said mass to controlled pyrolysis until the organic residue contains at least 90% carbon by weight, and said calcium formate is converted to calcium carbonate, to produce a pyrolysed product with said calcium carbonate homogeneously dispersed therein, and thereafter dispersing in the pyrolysed product a further combustion modifying agent which is at least one of ammonium di- hydrogen phosphate, diammonium hydrogen phosphate, the mono- , di- and tri- phosphates of sodium and potassium, and the meta- and tetra-borates of sodium and potassium, by contacting said pyrolysed product with a solution of said further combustion modifying agent, wherein said calcium formate and said further combustion modifying agent are dispersed on said fibres in said mass by dipping said mass in . a solution of said calcium formate, and subsequently deliquoring and drying said fibres, and by dipping said pyrolysed mass in a solution of said further combustion modifying agent, and subsequently deliquoring and drying said pyrolysed mass.
Claim 20
Dependent Claim
81 words
A tobacco substitute smoking product fuel, said fuel comprising pyrolysed viscose fibres having a carbon content of at least 90% carbon by weight of the organic pyrolysis residue, and having calcium carbonate homogeneously dispersed therein as an inorganic combustion modifying agent, wherein said fuel additionally contains a further combustion modifying agent which is at least one of ammonium dihydrogen phosphate; diammonium hydrogen phosphate; the mono-, di- and tri-phosphates of sodium and potassium; and the meta- and tetra-borates of sodium and potassium.
Claim 21
Dependent Claim
81 words
A tobacco substitute smoking product fuel, said fuel comprising pyrolysed viscose fibres having a carbon content of at least 90% carbon by weight of the organic pyrolysis residue, and having calcium carbonate homogeneously dispersed therein as an inorganic combustion modifying agent, wherein said fuel additionally contains a further combustion modifying agent which is at least one of ammonium dihydrogen phosphate; diammonium hydrogen phosphate; the mono-, di- and tri-phosphates of sodium and potassium; and the meta- and tetra-borates of sodium and potassium.
References Cited (Backward Citations)
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